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Field guide8 Curing Problems: How to Diagnose, Fix, and Prevent Them
Concept

Calibration, Metrology and Measurement Traceability

The system for relating process measurements to stated references through documented calibrations, known uncertainty, instrument status and decisions about fitness for purpose.

A measurement is useful only when its measurand, method, range and decision are clear. Temperature, mass, humidity, pH and water activity require different instruments and uncertainty expectations.

Calibration establishes the relation between indication and reference values; adjustment changes the device; verification checks whether defined requirements are met. These activities should not be treated as interchangeable labels.

Traceability requires a documented, unbroken chain of calibrations to appropriate references, with uncertainty considered at each step. A traceable result is not automatically suitable for every production limit.

Display resolution can be finer than actual accuracy. Selection should consider the tolerance around the process limit, environmental effects, sampling variation and the consequence of a wrong release decision.

Each instrument needs identity, status, interval, location or use and records. When a device is found out of tolerance, earlier product or process decisions that relied on it require impact assessment.

Reference materials, check devices, service providers, acceptance criteria and records should form one controlled system. The objective is defensible measurement, not certificates collected without connection to use.

Related in the Codex

References

  • https://www.nist.gov/calibrations/traceability
  • https://www.fao.org/fao-who-codexalimentarius/sh-proxy/en/?lnk=1&url=https%253A%252F%252Fworkspace.fao.org%252Fsites%252Fcodex%252FStandards%252FCXC%2B1-1969%252FCXC_001e.pdf
  • https://www.fao.org/fao-who-codexalimentarius/sh-proxy/en/?lnk=1&url=https%253A%252F%252Fworkspace.fao.org%252Fsites%252Fcodex%252FStandards%252FCXC%2B58-2005%252FCXC_058e.pdf